Relationship between enamel bond fatigue durability and surface free-energy characteristics with universal adhesives

Yuko Nagura, Akimasa Tsujimoto, Wayne W. Barkmeier, Hidehiko Watanabe, William W. Johnson, Toshiki Takamizawa, Mark A. Latta, Masashi Miyazaki

Research output: Contribution to journalArticle

3 Scopus citations

Abstract

The relationship between enamel bond fatigue durability and surface free-energy characteristics with universal adhesives was investigated. The initial shear bond strengths and shear fatigue strengths of five universal adhesives to enamel were determined with and without phosphoric acid pre-etching. The surface free-energy characteristics of adhesive-treated enamel with and without pre-etching were also determined. The initial shear bond strength and shear fatigue strength of universal adhesive to pre-etched enamel were higher than those to ground enamel. The initial shear bond strength and shear fatigue strength of universal adhesive to pre-etched enamel were material dependent, unlike those to ground enamel. The surface free-energy of the solid (γS) and the hydrogen-bonding force (γSh) of universal adhesive-treated enamel were different depending on the adhesive, regardless of the presence or absence of pre-etching. The bond fatigue durability of universal adhesives was higher to pre-etched enamel than to ground enamel. In addition, the bond fatigue durability to pre-etched enamel was material dependent, unlike that to ground enamel. The surface free-energy characteristics of universal adhesive-treated enamel were influenced by the adhesive type, regardless of the presence or absence of pre-etching. The surface free-energy characteristics of universal adhesive-treated enamel were related to the results of the bond fatigue durability.

Original languageEnglish (US)
JournalEuropean Journal of Oral Sciences
DOIs
StateAccepted/In press - Jan 1 2018

Keywords

  • Dental bonding
  • Dental debonding
  • Dental etching
  • Dental restoration failure

ASJC Scopus subject areas

  • Dentistry(all)

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    Nagura, Y., Tsujimoto, A., Barkmeier, W. W., Watanabe, H., Johnson, W. W., Takamizawa, T., Latta, M. A., & Miyazaki, M. (Accepted/In press). Relationship between enamel bond fatigue durability and surface free-energy characteristics with universal adhesives. European Journal of Oral Sciences. https://doi.org/10.1111/eos.12398